TA Instruments

AR1763-0001f

15/03/2013 17:00:14

Sample name	DI 40 mm AL P60 20 mm gap
Sample notes	 
Experiment notes	DI Deionised water, 40 mm diameter. 70 mm total depth of water, 20 mm gap, with PE beads
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1763
Run number	1 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	15/03/2013 17:00:14

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	Yes
Initial temperature	20.0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:00:30 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 3.000 rad/s
End controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 300.0 rad/s
End controlled variable	velocity 3.000 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	20.0 C
Set temperature system idle	No

Geometry name	25mm ETC AL plate with studs
Geometry notes	Standard ETC AL parallel plate with studs
Geometry material	Aluminum
Parallel plate diameter	25.00 mm
gap	20000 micro m
Gap offset	0 micro m
Geometry inertia	2.056 micro N.m.s^2
Geometry compliance	3.130E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	0.6250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	5.215E5 1/m^3
Fluid density factor	2.557E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	26500 micro m
Approximate sample volume	9.82 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0.6 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.261 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	1
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	21.01 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Continuous ramp step 1

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

0.99600	4.829	-133.10	20000	20.0	6.087	30.996	-43.38	3.018	-14.37	24800	2.3037	2723	1.4398	143.98	3.411E-3	0.0	0.5
1.9960	10.20	13.820	20000	20.0	6.087	31.996	4.505	6.373	0.7068	24800	13.8300	610.6	8.6438	864.38	3.411E-3	0.0	0.5
2.9960	15.66	26.038	20000	20.0	6.085	32.996	8.487	9.787	0.8672	24790	27.4034	258.8	17.127	1712.7	3.411E-3	0.0	0.5
3.9960	18.56	34.338	20000	20.0	6.085	33.996	11.19	11.60	0.9648	24790	41.3358	184.2	25.835	2583.5	3.411E-3	0.1	0.6
4.9960	24.77	54.973	20000	20.0	6.088	34.996	17.92	15.48	1.157	24800	68.0921	103.5	42.558	4255.8	3.411E-3	0.1	0.6
6.0120	31.66	85.181	20000	20.0	6.089	36.012	27.76	19.79	1.403	24810	107.1540	63.35	66.971	6697.1	3.411E-3	0.1	0.6
6.9960	34.10	96.814	20000	20.0	6.087	36.996	31.56	21.31	1.481	24800	126.8110	54.60	79.257	7925.7	3.411E-3	0.1	0.6
8.0120	39.37	125.52	20000	20.0	6.088	38.012	40.91	24.60	1.663	24810	165.7690	40.98	103.61	10361	3.411E-3	0.1	0.6
9.0520	46.08	168.33	20000	20.0	6.088	39.052	54.87	28.80	1.905	24800	223.8390	29.90	139.90	13990	3.411E-3	0.2	0.7
9.9960	51.00	202.50	20000	20.0	6.085	39.996	66.00	31.87	2.071	24790	275.1710	24.41	171.98	17198	3.411E-3	0.2	0.7
10.996	55.76	239.96	20000	20.0	6.087	40.996	78.21	34.85	2.244	24800	326.5260	20.42	204.08	20408	3.411E-3	0.2	0.7
11.996	60.13	278.17	20000	20.0	6.086	41.996	90.67	37.58	2.413	24790	377.8980	17.56	236.19	23619	3.411E-3	0.2	0.7
12.996	64.44	316.69	20000	20.0	6.086	42.996	103.2	40.27	2.563	24800	435.1850	15.29	271.99	27199	3.411E-3	0.2	0.7
13.996	69.17	362.23	20000	20.0	6.085	43.996	118.1	43.23	2.731	24790	498.9910	13.26	311.87	31187	3.411E-3	0.2	0.7
14.996	75.70	432.39	20000	20.0	6.080	44.996	140.9	47.32	2.979	24770	594.5710	11.06	371.61	37161	3.411E-3	0.2	0.7
16.012	79.95	474.99	20000	20.0	6.080	46.012	154.8	49.97	3.098	24770	665.2160	9.921	415.76	41576	3.411E-3	0.3	0.8
16.996	84.55	529.89	20000	20.0	6.079	46.996	172.7	52.84	3.269	24770	741.2440	8.870	463.28	46328	3.411E-3	0.3	0.8
17.992	91.00	610.87	20000	20.0	6.079	47.992	199.1	56.87	3.501	24770	855.7840	7.657	534.86	53487	3.411E-3	0.3	0.8
18.996	95.05	664.42	20000	20.0	6.078	48.996	216.6	59.40	3.646	24760	932.0850	7.017	582.55	58255	3.411E-3	0.3	0.8
19.992	99.42	721.34	20000	20.0	6.073	49.992	235.1	62.14	3.784	24740	1021.1700	6.409	638.23	63823	3.411E-3	0.3	0.8
21.012	105.8	808.16	20000	20.0	6.068	51.012	263.4	66.15	3.982	24720	1154.6000	5.649	721.63	72163	3.411E-3	0.4	0.9
22.008	109.9	871.31	20000	20.0	6.058	52.008	284.0	68.69	4.134	24680	1242.3700	5.231	776.48	77648	3.411E-3	0.4	0.9
22.996	114.2	936.91	20000	20.0	6.055	52.996	305.4	71.41	4.277	24670	1348.4800	4.838	842.80	84280	3.411E-3	0.4	0.9
24.000	120.7	1036.6	20000	20.0	6.042	54.000	337.9	75.41	4.481	24620	1495.8400	4.329	934.90	93490	3.411E-3	0.4	0.9
25.000	124.7	1102.7	20000	20.0	6.039	55.000	359.4	77.96	4.610	24610	1597.2500	4.048	998.28	99828	3.411E-3	0.4	0.9
26.000	129.1	1177.4	20000	20.0	6.029	56.000	383.8	80.67	4.758	24560	1712.0601	3.775	1070.0	1.0700E5	3.411E-3	0.4	0.9
26.996	135.5	1288.3	20000	20.0	6.012	56.996	419.9	84.66	4.960	24500	1882.0900	3.418	1176.3	1.1763E5	3.411E-3	0.4	0.9
27.992	139.6	1352.4	20000	20.0	6.007	57.992	440.8	87.22	5.054	24470	1995.9900	3.217	1247.5	1.2475E5	3.411E-3	0.5	1.0
28.996	143.7	1421.7	20000	20.0	5.972	58.996	463.4	89.78	5.161	24330	2116.3101	3.019	1322.7	1.3227E5	3.411E-3	0.5	1.0
30.132	150.0	1498.5	20000	20.0	5.906	60.132	488.4	93.78	5.209	24060	2306.0701	2.736	1441.3	1.4413E5	3.411E-3	0.5	1.0
31.008	154.2	1583.0	20000	20.0	5.895	61.008	516.0	96.35	5.355	24020	2433.1899	2.587	1520.7	1.5207E5	3.411E-3	0.5	1.0
32.000	158.3	1657.3	20000	20.0	5.883	62.000	540.2	98.92	5.461	23970	2565.2000	2.450	1603.3	1.6033E5	3.411E-3	0.5	1.0
32.992	164.7	1785.0	20000	20.0	5.846	62.992	581.8	102.9	5.654	23820	2774.5300	2.249	1734.1	1.7341E5	3.411E-3	0.5	1.0
34.008	168.8	1865.5	20000	20.0	5.848	64.008	608.0	105.5	5.764	23830	2913.2600	2.141	1820.8	1.8208E5	3.411E-3	0.6	1.1
34.996	174.9	1996.4	20000	20.0	5.816	64.996	650.7	109.3	5.954	23700	3127.6799	1.983	1954.8	1.9548E5	3.411E-3	0.6	1.1
35.996	179.1	2111.4	20000	20.0	5.815	65.996	688.2	111.9	6.148	23690	3279.2500	1.890	2049.5	2.0495E5	3.411E-3	0.6	1.1
37.000	183.3	2193.4	20000	20.0	5.800	67.000	714.9	114.5	6.242	23630	3431.9800	1.801	2145.0	2.1450E5	3.411E-3	0.6	1.1
38.016	189.3	2325.9	20000	20.0	5.770	68.016	758.1	118.3	6.407	23510	3658.1299	1.679	2286.3	2.2863E5	3.411E-3	0.6	1.1
38.992	193.5	2429.3	20000	20.0	5.754	68.992	791.8	120.9	6.549	23450	3822.3401	1.604	2389.0	2.3890E5	3.411E-3	0.6	1.1
40.012	199.7	2572.8	20000	20.0	5.755	70.012	838.6	124.8	6.720	23450	4068.7100	1.506	2542.9	2.5429E5	3.411E-3	0.7	1.2
40.996	203.7	2671.0	20000	20.0	5.706	70.996	870.6	127.3	6.839	23250	4232.7700	1.434	2645.5	2.6455E5	3.411E-3	0.7	1.2
42.000	207.9	2763.4	20000	20.0	5.687	72.000	900.7	129.9	6.933	23170	4409.4600	1.373	2755.9	2.7559E5	3.411E-3	0.7	1.2
42.996	214.1	2950.2	20000	20.0	5.688	72.996	961.6	133.8	7.187	23180	4676.1699	1.295	2922.6	2.9226E5	3.411E-3	0.7	1.2
44.000	218.1	3060.5	20000	20.0	5.667	74.000	997.6	136.3	7.317	23090	4851.3398	1.242	3032.1	3.0321E5	3.411E-3	0.7	1.2
44.996	224.3	3226.7	20000	20.0	5.645	74.996	1052	140.2	7.504	23000	5128.8901	1.171	3205.6	3.2056E5	3.411E-3	0.7	1.2
45.996	228.4	3318.4	20000	20.0	5.622	75.996	1082	142.8	7.577	22900	5318.2900	1.124	3323.9	3.3239E5	3.411E-3	0.8	1.3
47.012	234.5	3526.8	20000	20.0	5.668	77.012	1150	146.5	7.845	23090	5602.0898	1.075	3501.3	3.5013E5	3.411E-3	0.8	1.3
47.996	238.5	3614.1	20000	20.0	5.593	77.996	1178	149.1	7.902	22790	5797.8398	1.025	3623.6	3.6237E5	3.411E-3	0.8	1.3
48.996	242.7	3723.8	20000	20.0	5.579	78.996	1214	151.7	8.003	22730	5999.6299	0.9881	3749.8	3.7498E5	3.411E-3	0.8	1.3
49.996	248.8	3861.4	20000	20.0	5.496	79.996	1259	155.5	8.095	22390	6303.3398	0.9264	3939.6	3.9396E5	3.411E-3	0.8	1.3
50.996	252.8	4059.4	20000	20.0	5.563	80.996	1323	158.0	8.375	22670	6511.5000	0.9081	4069.7	4.0697E5	3.411E-3	0.8	1.3
52.012	259.0	4194.7	20000	20.0	5.485	82.012	1367	161.9	8.446	22350	6834.1401	0.8527	4271.3	4.2713E5	3.411E-3	0.9	1.4
53.008	263.1	4358.7	20000	20.0	5.489	83.008	1421	164.4	8.641	22360	7048.5200	0.8273	4405.3	4.4053E5	3.411E-3	0.9	1.4
53.996	269.1	4574.7	20000	20.0	5.502	83.996	1491	168.2	8.865	22420	7378.9600	0.7923	4611.9	4.6119E5	3.411E-3	0.9	1.4
55.012	273.3	4630.1	20000	20.0	5.406	85.012	1509	170.8	8.836	22030	7601.7998	0.7550	4751.1	4.7511E5	3.411E-3	0.9	1.4
55.996	277.4	4816.6	20000	20.0	5.461	85.996	1570	173.3	9.057	22250	7828.8301	0.7405	4893.0	4.8930E5	3.411E-3	0.9	1.4
57.000	283.4	5065.0	20000	20.0	5.467	87.000	1651	177.1	9.322	22270	8168.6001	0.7101	5105.4	5.1054E5	3.411E-3	1.0	1.5
57.996	287.5	5130.7	20000	20.0	5.315	87.996	1672	179.7	9.308	21650	8409.4004	0.6708	5255.9	5.2559E5	3.411E-3	1.0	1.5
59.020	293.6	5368.2	20000	20.0	5.344	89.020	1750	183.5	9.537	21770	8767.5098	0.6468	5479.7	5.4797E5	3.411E-3	1.0	1.5
60.008	297.6	5481.2	20000	20.0	5.322	90.008	1787	186.0	9.606	21680	9008.1201	0.6269	5630.1	5.6301E5	3.411E-3	1.0	1.5

Peak hold step

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0080	300.0	5524.0	20000	20.0	5.242	92.008	1801	187.5	9.602	21360	274.6860	0.6074	171.68	17168	3.411E-3	0.0	1.5
2.0200	300.0	5635.3	20000	20.0	5.393	93.020	1837	187.5	9.796	21970	528.1880	0.6249	330.12	33012	3.411E-3	0.0	1.6
3.0040	300.0	5551.5	20000	20.0	5.179	94.004	1809	187.5	9.651	21100	902.9670	0.6002	564.35	56435	3.411E-3	0.1	1.6
4.0040	300.0	5564.3	20000	20.0	5.271	95.004	1814	187.5	9.673	21470	1154.2400	0.6108	721.40	72140	3.411E-3	0.1	1.6
5.0080	300.0	5524.3	20000	20.0	5.187	96.008	1801	187.5	9.604	21140	1405.7300	0.6012	878.58	87858	3.411E-3	0.1	1.6
6.0440	300.0	5495.4	20000	20.0	5.164	97.044	1791	187.5	9.553	21040	1783.8500	0.5984	1114.9	1.1149E5	3.411E-3	0.1	1.6
7.0360	300.0	5589.1	20000	20.0	5.224	98.036	1822	187.5	9.716	21280	2038.0900	0.6055	1273.8	1.2738E5	3.411E-3	0.1	1.6
8.0280	300.0	5552.6	20000	20.0	5.262	99.028	1810	187.5	9.653	21440	2410.9199	0.6098	1506.8	1.5068E5	3.411E-3	0.1	1.7
9.0200	300.0	5537.0	20000	20.0	5.206	100.020	1805	187.5	9.627	21210	2674.6899	0.6035	1671.7	1.6717E5	3.411E-3	0.2	1.7
10.000	300.0	5510.5	20000	20.0	5.165	101.000	1796	187.5	9.579	21040	2916.3501	0.5986	1822.7	1.8227E5	3.411E-3	0.2	1.7
11.004	300.0	5498.9	20000	20.0	5.191	102.004	1792	187.5	9.559	21150	3294.3501	0.6016	2059.0	2.0590E5	3.411E-3	0.2	1.7
12.024	300.0	5589.2	20000	20.0	5.320	103.024	1822	187.5	9.715	21670	3543.3301	0.6164	2214.6	2.2146E5	3.411E-3	0.2	1.7
13.028	300.0	5544.1	20000	20.0	5.242	104.028	1807	187.5	9.638	21360	3918.8601	0.6076	2449.3	2.4493E5	3.411E-3	0.2	1.7
14.020	300.0	5597.9	20000	20.0	5.267	105.020	1825	187.5	9.731	21460	4170.2002	0.6104	2606.4	2.6064E5	3.411E-3	0.2	1.8
15.020	300.0	5557.9	20000	20.0	5.243	106.020	1812	187.5	9.662	21360	4421.7002	0.6076	2763.6	2.7636E5	3.411E-3	0.3	1.8
16.004	300.0	5530.1	20000	20.0	5.262	107.004	1803	187.5	9.613	21440	4798.4800	0.6098	2999.1	2.9991E5	3.411E-3	0.3	1.8
17.004	300.0	5583.9	20000	20.0	5.262	108.004	1820	187.5	9.707	21440	5053.6299	0.6098	3158.5	3.1585E5	3.411E-3	0.3	1.8
18.024	300.0	5507.2	20000	20.0	5.291	109.024	1795	187.5	9.575	21560	5428.3101	0.6133	3392.7	3.3927E5	3.411E-3	0.3	1.8
19.004	300.0	5554.3	20000	20.0	5.259	110.004	1810	187.5	9.656	21430	5678.2900	0.6095	3548.9	3.5489E5	3.411E-3	0.3	1.8
20.016	300.0	5536.0	20000	20.0	5.243	111.016	1804	187.5	9.624	21360	5930.7202	0.6076	3706.7	3.7067E5	3.411E-3	0.3	1.9
21.004	300.0	5554.7	20000	20.0	5.272	112.004	1811	187.5	9.657	21480	6306.6099	0.6110	3941.6	3.9416E5	3.411E-3	0.4	1.9
22.004	300.0	5548.6	20000	20.0	5.270	113.004	1809	187.5	9.646	21470	6559.6201	0.6107	4099.8	4.0998E5	3.411E-3	0.4	1.9
23.004	300.0	5546.3	20000	20.0	5.225	114.004	1808	187.5	9.642	21290	6809.1802	0.6055	4255.7	4.2557E5	3.411E-3	0.4	1.9
24.004	300.0	5603.2	20000	20.0	5.250	115.004	1826	187.5	9.740	21390	7186.0601	0.6085	4491.3	4.4913E5	3.411E-3	0.4	1.9
25.024	300.0	5568.1	20000	20.0	5.233	116.024	1815	187.5	9.679	21320	7438.5801	0.6064	4649.1	4.6491E5	3.411E-3	0.4	1.9
26.012	300.0	5551.7	20000	20.0	5.179	117.012	1810	187.5	9.651	21100	7814.5601	0.6002	4884.1	4.8841E5	3.411E-3	0.4	2.0
27.004	300.0	5571.4	20000	20.0	5.224	118.004	1816	187.5	9.685	21280	8068.2998	0.6054	5042.7	5.0427E5	3.411E-3	0.5	2.0
28.004	300.0	5568.2	20000	20.0	5.250	119.004	1815	187.5	9.680	21390	8317.3799	0.6085	5198.4	5.1984E5	3.411E-3	0.5	2.0
29.004	300.0	5552.2	20000	20.0	5.295	120.004	1810	187.5	9.652	21570	8694.0303	0.6136	5433.8	5.4338E5	3.411E-3	0.5	2.0
30.004	300.0	5574.9	20000	20.0	5.252	121.004	1817	187.5	9.692	21400	8945.5098	0.6088	5590.9	5.5909E5	3.411E-3	0.5	2.0
31.076	300.0	5633.5	20000	20.0	5.333	122.076	1836	187.5	9.793	21730	9323.7402	0.6180	5827.3	5.8273E5	3.411E-3	0.5	2.0
32.020	300.0	5543.6	20000	20.0	5.242	123.020	1807	187.5	9.637	21360	9573.7803	0.6075	5983.6	5.9836E5	3.411E-3	0.5	2.1
33.004	300.0	5593.2	20000	20.0	5.367	124.004	1823	187.5	9.722	21870	9826.7500	0.6219	6141.7	6.1417E5	3.411E-3	0.6	2.1
34.004	300.0	5565.2	20000	20.0	5.310	125.004	1814	187.5	9.674	21640	10204.300	0.6154	6377.7	6.3777E5	3.411E-3	0.6	2.1
35.020	300.0	5554.9	20000	20.0	5.225	126.020	1811	187.5	9.656	21290	10455.000	0.6054	6534.4	6.5344E5	3.411E-3	0.6	2.1
36.024	300.0	5592.8	20000	20.0	5.238	127.024	1823	187.5	9.722	21340	10833.900	0.6071	6771.2	6.7712E5	3.411E-3	0.6	2.1
37.000	300.0	5642.0	20000	20.0	5.334	128.000	1839	187.5	9.808	21730	11084.500	0.6181	6927.8	6.9278E5	3.411E-3	0.6	2.1
38.004	300.0	5558.7	20000	20.0	5.264	129.004	1812	187.5	9.664	21450	11333.700	0.6102	7083.6	7.0836E5	3.411E-3	0.6	2.2
39.020	300.0	5518.1	20000	20.0	5.264	130.020	1799	187.5	9.592	21450	11715.200	0.6100	7322.0	7.3220E5	3.411E-3	0.7	2.2
40.044	300.0	5558.3	20000	20.0	5.310	131.044	1812	187.5	9.662	21630	11961.900	0.6153	7476.2	7.4762E5	3.411E-3	0.7	2.2
41.004	300.0	5549.1	20000	20.0	5.217	132.004	1809	187.5	9.648	21260	12212.800	0.6048	7633.0	7.6330E5	3.411E-3	0.7	2.2
42.016	300.0	5545.0	20000	20.0	5.207	133.016	1807	187.5	9.639	21210	12589.600	0.6034	7868.5	7.8685E5	3.411E-3	0.7	2.2
43.008	300.0	5480.1	20000	20.0	5.237	134.008	1786	187.5	9.527	21340	12841.300	0.6069	8025.8	8.0258E5	3.411E-3	0.7	2.2
44.012	300.0	5528.6	20000	20.0	5.264	135.012	1802	187.5	9.611	21450	13219.900	0.6101	8262.4	8.2624E5	3.411E-3	0.7	2.3
45.008	300.0	5501.2	20000	20.0	5.197	136.008	1793	187.5	9.563	21170	13469.600	0.6023	8418.5	8.4185E5	3.411E-3	0.8	2.3
46.012	300.0	5528.6	20000	20.0	5.205	137.012	1802	187.5	9.611	21210	13720.800	0.6033	8575.5	8.5755E5	3.411E-3	0.8	2.3
47.008	300.0	5516.6	20000	20.0	5.213	138.008	1798	187.5	9.590	21240	14097.600	0.6041	8811.0	8.8110E5	3.411E-3	0.8	2.3
48.016	300.0	5548.9	20000	20.0	5.350	139.016	1809	187.5	9.646	21800	14349.700	0.6199	8968.6	8.9686E5	3.411E-3	0.8	2.3
49.020	300.0	5566.0	20000	20.0	5.301	140.020	1814	187.5	9.676	21600	14600.400	0.6144	9125.3	9.1253E5	3.411E-3	0.8	2.3
50.076	300.0	5554.7	20000	20.0	5.306	141.076	1811	187.5	9.656	21620	14977.300	0.6150	9360.8	9.3608E5	3.411E-3	0.8	2.4
51.020	300.0	5546.6	20000	20.0	5.222	142.020	1808	187.5	9.642	21280	15228.600	0.6052	9517.9	9.5179E5	3.411E-3	0.9	2.4
52.004	300.0	5520.1	20000	20.0	5.201	143.004	1799	187.5	9.596	21190	15605.800	0.6028	9753.6	9.7536E5	3.411E-3	0.9	2.4
53.020	300.0	5507.9	20000	20.0	5.182	144.020	1795	187.5	9.574	21110	15856.800	0.6005	9910.5	9.9105E5	3.411E-3	0.9	2.4
54.020	300.0	5528.2	20000	20.0	5.268	145.020	1802	187.5	9.610	21460	16108.400	0.6105	10068	1.0068E6	3.411E-3	0.9	2.4
55.004	300.0	5504.3	20000	20.0	5.210	146.004	1794	187.5	9.569	21230	16485.400	0.6038	10303	1.0303E6	3.411E-3	0.9	2.4
56.004	300.0	5560.6	20000	20.0	5.252	147.004	1812	187.5	9.667	21400	16736.600	0.6088	10460	1.0460E6	3.411E-3	0.9	2.5
57.004	300.0	5589.6	20000	20.0	5.306	148.004	1822	187.5	9.716	21620	17114.100	0.6148	10696	1.0696E6	3.411E-3	1.0	2.5
58.020	300.0	5522.5	20000	20.0	5.192	149.020	1800	187.5	9.600	21150	17365.000	0.6017	10853	1.0853E6	3.411E-3	1.0	2.5
59.016	300.0	5545.7	20000	20.0	5.222	150.016	1808	187.5	9.641	21280	17618.500	0.6053	11012	1.1012E6	3.411E-3	1.0	2.5
60.020	300.0	5589.6	20000	20.0	5.219	151.020	1822	187.5	9.717	21260	17993.301	0.6048	11246	1.1246E6	3.411E-3	1.0	2.5

Continuous ramp step 2

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0040	296.5	5407.7	20000	20.0	5.252	152.004	1763	185.3	9.510	21400	288.0940	0.6229	180.06	18006	3.411E-3	0.0	2.5
2.0080	292.5	5255.1	20000	20.0	5.214	153.008	1713	182.8	9.368	21240	526.3280	0.6355	328.96	32896	3.411E-3	0.0	2.6
3.0040	286.4	5063.9	20000	20.0	5.318	154.004	1651	179.0	9.222	21670	883.7040	0.6763	552.32	55232	3.411E-3	0.1	2.6
4.0200	282.3	4926.5	20000	20.0	5.358	155.020	1606	176.4	9.103	21830	1121.1700	0.7015	700.73	70073	3.411E-3	0.1	2.6
5.0040	276.2	4761.4	20000	20.0	5.352	156.004	1552	172.6	8.990	21810	1460.2800	0.7317	912.68	91268	3.411E-3	0.1	2.6
6.0200	272.1	4565.0	20000	20.0	5.375	157.020	1488	170.1	8.748	21900	1684.8600	0.7570	1053.0	1.0530E5	3.411E-3	0.1	2.6
7.0000	268.0	4469.4	20000	20.0	5.465	158.000	1457	167.5	8.697	22270	1909.9800	0.7936	1193.7	1.1937E5	3.411E-3	0.1	2.6
8.0040	262.0	4280.6	20000	20.0	5.449	159.004	1395	163.7	8.521	22200	2230.4700	0.8281	1394.0	1.3940E5	3.411E-3	0.1	2.7
9.0040	257.9	4149.7	20000	20.0	5.479	160.004	1353	161.2	8.390	22320	2446.5300	0.8590	1529.1	1.5291E5	3.411E-3	0.2	2.7
10.004	251.7	3947.3	20000	20.0	5.451	161.004	1287	157.3	8.178	22210	2761.3701	0.8973	1725.9	1.7259E5	3.411E-3	0.2	2.7
11.016	247.7	3822.2	20000	20.0	5.497	162.016	1246	154.8	8.048	22390	2961.7100	0.9345	1851.1	1.8511E5	3.411E-3	0.2	2.7
12.004	241.6	3674.2	20000	20.0	5.503	163.004	1198	151.0	7.931	22420	3263.4600	0.9835	2039.7	2.0397E5	3.411E-3	0.2	2.7
13.020	237.5	3565.9	20000	20.0	5.587	164.020	1162	148.4	7.830	22770	3462.4700	1.033	2164.0	2.1640E5	3.411E-3	0.2	2.7
14.004	233.3	3426.6	20000	20.0	5.606	165.004	1117	145.8	7.659	22840	3660.4099	1.074	2287.8	2.2878E5	3.411E-3	0.2	2.8
15.020	227.3	3264.0	20000	20.0	5.598	166.020	1064	142.1	7.489	22810	3937.9800	1.130	2461.2	2.4612E5	3.411E-3	0.3	2.8
16.004	223.2	3163.4	20000	20.0	5.646	167.004	1031	139.5	7.393	23000	4125.6401	1.183	2578.5	2.5785E5	3.411E-3	0.3	2.8
17.004	217.1	3002.7	20000	20.0	5.682	168.004	978.7	135.7	7.215	23150	4394.6899	1.258	2746.7	2.7467E5	3.411E-3	0.3	2.8
18.000	213.0	2883.4	20000	20.0	5.656	169.000	939.8	133.1	7.060	23040	4571.1401	1.301	2857.0	2.8570E5	3.411E-3	0.3	2.8
19.004	208.9	2785.7	20000	20.0	5.699	170.004	908.0	130.6	6.955	23220	4744.9199	1.362	2965.6	2.9656E5	3.411E-3	0.3	2.8
20.004	202.7	2603.7	20000	20.0	5.683	171.004	848.7	126.7	6.700	23160	5001.2798	1.443	3125.8	3.1258E5	3.411E-3	0.3	2.9
21.076	198.7	2545.6	20000	20.0	5.740	172.076	829.7	124.2	6.683	23390	5164.2402	1.517	3227.7	3.2277E5	3.411E-3	0.4	2.9
22.016	192.5	2370.1	20000	20.0	5.735	173.016	772.5	120.3	6.422	23370	5407.7500	1.615	3379.8	3.3798E5	3.411E-3	0.4	2.9
23.044	188.2	2291.4	20000	20.0	5.785	174.044	746.9	117.6	6.349	23570	5571.5098	1.703	3482.2	3.4822E5	3.411E-3	0.4	2.9
24.004	184.1	2192.5	20000	20.0	5.792	175.004	714.6	115.1	6.210	23600	5797.8101	1.782	3623.6	3.6236E5	3.411E-3	0.4	2.9
25.016	178.0	2038.8	20000	20.0	5.803	176.016	664.5	111.3	5.973	23640	5946.2500	1.910	3716.4	3.7164E5	3.411E-3	0.4	2.9
25.996	173.8	1954.6	20000	20.0	5.812	176.996	637.1	108.6	5.866	23680	6096.1299	2.007	3810.1	3.8101E5	3.411E-3	0.4	2.9
27.020	167.7	1852.9	20000	20.0	5.872	178.020	604.0	104.8	5.762	23920	6301.5601	2.177	3938.5	3.9385E5	3.411E-3	0.5	3.0
28.004	163.6	1751.9	20000	20.0	5.850	179.004	571.0	102.2	5.585	23840	6438.9600	2.280	4024.4	4.0244E5	3.411E-3	0.5	3.0
29.004	159.4	1652.0	20000	20.0	5.865	180.004	538.5	99.62	5.405	23900	6577.7402	2.408	4111.1	4.1111E5	3.411E-3	0.5	3.0
30.020	153.2	1533.3	20000	20.0	5.916	181.020	499.8	95.73	5.221	24110	6770.0200	2.630	4231.3	4.2313E5	3.411E-3	0.5	3.0
31.000	149.1	1456.7	20000	20.0	5.901	182.000	474.8	93.17	5.096	24040	6894.8701	2.770	4309.3	4.3093E5	3.411E-3	0.5	3.0
32.004	142.7	1332.3	20000	20.0	5.907	183.004	434.2	89.20	4.868	24070	7082.1699	3.025	4426.4	4.4264E5	3.411E-3	0.5	3.1
33.044	138.4	1258.9	20000	20.0	5.915	184.044	410.3	86.52	4.743	24100	7201.0698	3.219	4500.7	4.5007E5	3.411E-3	0.6	3.1
34.020	134.4	1182.3	20000	20.0	5.931	185.020	385.4	83.97	4.589	24170	7312.8999	3.427	4570.6	4.5706E5	3.411E-3	0.6	3.1
35.024	128.0	1077.3	20000	20.0	5.948	186.024	351.2	80.01	4.389	24230	7481.1699	3.786	4675.7	4.6757E5	3.411E-3	0.6	3.1
36.016	123.7	1015.1	20000	20.0	5.963	187.016	330.9	77.32	4.279	24300	7587.2002	4.064	4742.0	4.7420E5	3.411E-3	0.6	3.1
37.020	119.7	952.85	20000	20.0	5.980	188.020	310.6	74.78	4.153	24360	7686.9702	4.356	4804.4	4.8044E5	3.411E-3	0.6	3.1
38.008	113.3	852.58	20000	20.0	5.993	189.008	277.9	70.81	3.925	24420	7836.4800	4.870	4897.8	4.8978E5	3.411E-3	0.6	3.2
39.008	109.0	793.89	20000	20.0	5.995	190.008	258.8	68.12	3.799	24430	7929.9399	5.263	4956.2	4.9562E5	3.411E-3	0.7	3.2
40.008	105.0	743.74	20000	20.0	5.996	191.008	242.4	65.60	3.695	24430	8017.1099	5.677	5010.7	5.0107E5	3.411E-3	0.7	3.2
41.016	98.60	662.48	20000	20.0	6.021	192.016	215.9	61.62	3.504	24530	8147.7300	6.460	5092.3	5.0923E5	3.411E-3	0.7	3.2
42.016	94.14	602.47	20000	20.0	6.026	193.016	196.4	58.84	3.338	24550	8234.6904	7.093	5146.7	5.1467E5	3.411E-3	0.7	3.2
43.004	89.96	546.15	20000	20.0	6.029	194.004	178.0	56.22	3.166	24560	8309.7900	7.771	5193.6	5.1936E5	3.411E-3	0.7	3.2
44.004	83.56	474.68	20000	20.0	6.032	195.004	154.7	52.23	2.962	24570	8422.7100	9.009	5264.2	5.2642E5	3.411E-3	0.7	3.3
45.060	79.03	425.38	20000	20.0	6.044	196.060	138.7	49.39	2.807	24620	8495.5098	10.09	5309.7	5.3097E5	3.411E-3	0.8	3.3
46.036	74.84	380.36	20000	20.0	6.048	197.036	124.0	46.78	2.650	24640	8558.4697	11.26	5349.0	5.3490E5	3.411E-3	0.8	3.3
47.020	68.41	323.54	20000	20.0	6.056	198.020	105.5	42.76	2.466	24680	8651.0703	13.50	5406.9	5.4069E5	3.411E-3	0.8	3.3
48.016	63.78	282.84	20000	20.0	6.061	199.016	92.19	39.86	2.313	24690	8712.2998	15.54	5445.2	5.4452E5	3.411E-3	0.8	3.3
49.004	59.56	244.75	20000	20.0	6.066	200.004	79.78	37.23	2.143	24720	8761.7500	17.83	5476.1	5.4761E5	3.411E-3	0.8	3.3
50.016	55.30	209.17	20000	20.0	6.068	201.016	68.18	34.56	1.973	24730	8811.1797	20.70	5507.0	5.5070E5	3.411E-3	0.8	3.4
51.020	50.70	179.10	20000	20.0	6.073	202.020	58.38	31.69	1.842	24740	8860.3301	24.65	5537.7	5.5377E5	3.411E-3	0.9	3.4
52.016	43.95	140.36	20000	20.0	6.080	203.016	45.75	27.47	1.666	24770	8921.7197	32.83	5576.1	5.5761E5	3.411E-3	0.9	3.4
53.000	39.59	114.35	20000	20.0	6.079	204.000	37.27	24.74	1.506	24770	8958.4697	40.46	5599.0	5.5990E5	3.411E-3	0.9	3.4
54.004	34.71	89.685	20000	20.0	6.086	205.004	29.23	21.70	1.347	24790	8994.9199	52.67	5621.8	5.6218E5	3.411E-3	0.9	3.4
55.000	29.59	69.093	20000	20.0	6.090	206.000	22.52	18.49	1.218	24810	9025.2100	72.56	5640.8	5.6408E5	3.411E-3	0.9	3.4
56.000	25.20	50.310	20000	20.0	6.089	207.000	16.40	15.75	1.041	24810	9049.3096	100.0	5655.8	5.6558E5	3.411E-3	0.9	3.5
57.000	19.96	33.563	20000	20.0	6.093	208.000	10.94	12.48	0.8769	24830	9073.6602	159.5	5671.0	5.6710E5	3.411E-3	1.0	3.5
58.004	14.06	17.738	20000	20.0	6.091	209.004	5.782	8.786	0.6581	24820	9090.3701	321.5	5681.5	5.6815E5	3.411E-3	1.0	3.5
59.000	11.82	13.161	20000	20.0	6.092	210.000	4.290	7.388	0.5806	24820	9096.0801	454.8	5685.0	5.6851E5	3.411E-3	1.0	3.5
60.004	6.649	4.6946	20000	20.0	6.093	211.004	1.530	4.156	0.3682	24820	9104.2402	1437	5690.2	5.6902E5	3.411E-3	1.0	3.5

